Sample submission
Dear user(s) of the micro-elemental analysis service
We are making a big effort to obtain optimum results. However, we need your help. Please follow the rules listed below to improve the results - it is in your own interest! If you have any questions, do not hesitate to contact us.
Rules:
- The sample must be homogeneous. Solutions can not be measured.
- Use clean test tubes from the „Schalter" (HCI Shop) only (chrome sulphuric acid, dest. water, alcohol, ether, HV)
- Label the test tubes with: name, group name, molecular formula, special identification and the elements which are to be determined.
- Fill in the Elemental-Analysis-formular completely.
- Contact us as soon as possible if the sample is sensitive to light and air.
- Solid material must be powdered and well-dried at minimum 24 h on high vacuum.
- If you don't know the exact molecular formula, please give us the expected Percentage of each Element.
- We reject analyses of samples if the test tubes are insufficiently labeled or formulars are incompletely filled out
Quantities:
Please give us plenty of substance. You will get back all the substance that is not required. If you are coming from outside DCHAB please make a remark so that we can give your sample back after measuring.
How to fill out the Elemental Analysis -Formular
Please fill in the form completely as shown in the example below. Especially important are the categories: melting point (measured yourself!), purification and drying are very important as well. If the sample is a commercial product, then note „purchased" in the line „purification".
ETH members have to use the original forms which are available in our laboratory, users from outside may Downloaddownload the form from the website (PDF, 55 KB).
Additionally, please label the sample as indicated below:
